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LCQ-Deca (ThermoElectron)

The LCQ-Deca is an ion-trap mass spectrometer with electrospray (ESI) ionization and MS/MS or MSnth capabilities. This instrument is primarily dedicated for protein ID, analysis of peptides, and other proteomics work, but is also utilized for LC/MS/MS of small-molecule samples that require LC introduction. It is equipped with a nanoLC system (Eksigent) and is routinely used for protein ID from in-gel digests and proteins from solution.

For applications of the instrument, see available services.

LCQ-Deca Performance and Capabilities

  • Nano-LC/MS/MS
  • < 0.5 Da mass error (full scan);
    <0.05 Da mass error (zoom scan)
  • Femtomole-range sensitivity (e.g. 2 femtomoles BSA digest injected on column)
  • MS/MS with CID fragmentation (for peptide sequencing or structure elucidation)

How the LCQ-Deca is Equipped

  • Nanospray or microspray ESI
  • NanoLC system (Eksigent Technologies) –
    • splitless gradients as low as 20 nl/min; 75um ID C18 column;
    • protein digests typically analyzed at a flow rate of 400nl/min
  • Collision-induced dissociation (CID) for MS/MS

The facility is also equipped with several other instruments:


 
 
 

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